▶ Watch On-Demand | 55 Minutes

On-Demand Session: Advanced Nanoscale Chemical Analysis using Photothermal AFM-IR & Correlated Mapping of Mechanical and Electrical Properties

View this on-demand webinar on advanced nanoscale analysis using photothermal AFM-IR spectroscopy. 
Watch Now | 22 Minutes

Part 1 - Technological and Hardware Background

Presented by Hartmut Stadler, Ph.D., Applications Engineer, Bruker (November 9, 2023)

PRESENTATION HIGHLIGHTS:

[00:00:00] Introduction to AFM

AFM Modes for Property Mapping

  • [00:03:10] PeakForce QNM
  • [00:06:13] AFM-nDMA
  • [00:09:25] PeakForce KPFM
  • [00:11:46] AFM-IR

[00:16:20] Hardware Configuration with Bruker's IconIR Scanning Probe Microscopy System

[00:18:30] Correlation of measurements (MIRO)

Watch Now | 24 Minutes

Part 2 - Application Examples

Presented by Chuzeng Li, Ph.D., Applications Engineer, Bruker (November 9, 2023)

PRESENTATION HIGHLIGHTS:

[00:00:00]Poly-Styrene & Low Density PolyEthylene Applications

  • [00:00:32] Point Spectroscopy to Reveal the Chemistry
  • [00:02:14] AFM-IR Maps to Show the Different Chemical Domains 
  • [00:02:55] Correlative nano-Mechanical, Electrical and Chemical Mapping

[00:05:25] Poly-Styrene-Butadiene Rubber Applications

  • [00:06:00] Mechanical Properties
  • [00:07:00] Chemical IR Map
  • [00:10:12] Photothermal AFM-IR

[00:11:30] Polymer blend of Poly-Carbonate-Poly Applications

  • [00:11:55] nDMA for Viscoelastic Properties
  • [00:17:30] AFM-IR DataCube for Hyperspectral Imaging
  • [00:07:00] Lithium Battery Cathode Example

[00:21:35] Summary

Watch Now | 8 Minutes

Q&A

       PRESENTATION HIGHLIGHTS:

  • [00:00:00] Is AFM-IR Destructive for the top layer of the sample? What is the effect of topography on IR absorption?
  • [00:02:10] What is the Z depth resolution of AFM-IR? Is there any way to modify or minimize it?
  • [00:03:30] Does it take 12 hours to record all AFM-IR Images?
  • [00:04:25] Which technique (mode or contact mode) provides a better lateral resolution tapping?
  • [00:04:50] What is the smallest size of structure that can be imaged chemically?
  • [00:06:21] In AFM-IR, is it possible to use tapping mode and infrared mapping simultaneously?
  • [00:06:54] Which platforms offered by Bruker offer AFM-IR?