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Characterization of Thin Dielectric Films with Atomic Force Microscopy

Learn how AFM can be applied to measure and quantify the properties of dielectric film.
Watch Now | 15 Minutes

Topography and Conductivity Based Measurements

Presented by Peter De Wolf, Ph.D., Worldwide Application Director, Bruker Nano Surfaces and Metrology (December 7, 2022)

       PRESENTATION HIGHLIGHTS:

  • [00:00:00] Introduction to the AFM technique
  • [00:01:09] Typical applications in dielectrics
  • [00:03:54] Electrical properties measurable by AFM
  • [00:04:53] Conductive AFM (C-AFM)
  • [00:06:29] Tunneling-AFM (TUNA)
  • [00:12:34] DataCube TUNA
Watch Now | 8 Minutes

Live Demo - Tunneling AFM on Dimension Icon AFM

Presented by Michael Febvre, Ph.D., Application Manager, Bruker EMEA (December 7, 2022)

       PRESENTATION HIGHLIGHTS:

  • [00:00:11] Instrument setup and sample
  • [00:01:30] Software configuration
  • [00:02:52] Data acquisition
  • [00:04:07] Generating an I-V curve
  • [00:05:54] Data images and interpretation
Watch Now | 12 Minutes

Charge and Capacitance Based Measurements

Presented by Peter De Wolf, Ph.D., Worldwide Application Director, Bruker Nano Surfaces and Metrology (December 7, 2022)

       PRESENTATION HIGHLIGHTS:

  • [00:00:14] Scanning Microwave Impedance Microscopy (sMIM)
  • [00:06:47] Kelvin Probe Force Microscopy (KPFM)
  • [00:09:15] Extract ε from capacitance measurements between the tip and sample
  • [00:10:40] Electrostatic Force Microscopy (EFM)
Watch Now | 9 Minutes

Live Demo - Scanning Microwave Impedance Microscopy on Dimension Icon AFM

Presented by Hartmut Stadler, Ph.D., Application Scientist, Bruker (December 7, 2022)

       PRESENTATION HIGHLIGHTS:

  • [00:00:00] Experimental setup
  • [00:02:16] Data acquisition
  • [00:05:14] Generating capacitance-distance curves
Watch Now | 7 Minutes

Advanced AFM Characterization

Presented by Peter De Wolf, Ph.D., Worldwide Application Director, Bruker Nano Surfaces and Metrology (December 7, 2022)

       PRESENTATION HIGHLIGHTS:

  • [00:00:11] Measurements on cross-sectioned devices
  • [00:00:59] PiezoResponse Force Microscopy (PFM)
  • [00:03:17] Chemical property characterization by AFM-IR
  • [00:05:58] Other techniques for characterizing dielectric materials
Watch Now | 9 Minutes

Q&A

Presented by Peter De Wolf, Ph.D., Worldwide Application Director, Bruker Nano Surfaces and Metrology and Andrea Slade, Ph.D., Product Manager, Materials AFM, Bruker Nano Surface & Metrology (December 7, 2022)

       PRESENTATION HIGHLIGHTS:

  • [00:00:00] What is the difference between C-AFM and TUNA and what is the maximum TUNA current?
  • [00:01:06] Can one get similar conductive AFM graphs on wide band gap semiconductors?
  • [00:01:48] How many I-V curves are recorded per pixel and is the I-V curve generated an average of multiple recordings?
  • [00:02:57] Are these kinds of conductivity measurements with TUNA also possible on materials that are less insulating or more bulky? (e.g., low band gap semiconductors, like silicon substrates or germanium)
  • [00:04:11] Is it possible to use KPFM to estimate the size of the depletion region in a PNP semiconductor device structure via the static charge distribution?
  • [00:05:51] What are the challenges for electrical measurements on softer samples and biological samples (e.g., neuronal cells that are also known to conduct electrical signals)?
  • [00:07:58] What materials can be detected by AFM-IR (on the Dimension IconIR system)?