BASIC - CP/MAS Course
(SB and WB Systems)

Info:

Introductory Course.

Topics:

• Basic theory of the interactions in solid state samples and the MAS technique.
• Introduction of the CP/MAS technique and heteronuclear decoupling techniques.
• Introduction to Solid State NMR of Spin ½ nuclei (e.g. 13C/15N/29Si/31P).
• Basic introduction to modern spectrometer concepts.
• Sample preparation and MAS–spinner handling.
• Setup and interpretation of 1D – CP/MAS experiments (how to check the probe / shimming /RF calibration / finding HH matching condition).
• Setup of variable temperature experiments.
• Setup and evaluation of relaxation measurements on X nuclei and protons.

Remarks:

This course is intended for users of standard-bore solid state NMR instruments with CP/MAS probes.

Prerequisite Qualification:

Basic knowledge of computer handling; the concept of NMR in general and the TOPSPIN software.

Date:

February 26^th - 29^th, 2024

Location: