Exploring the Limits of Viscoelastic Phenomena with AFM-Based Nanomechanics

Learn New Ways of Measuring Viscoelasticity with Atomic Force Microscopy

In this on-demand webinar, Exploring the Limits of Viscoelastic Phenomena with AFM-Based Nanomechanics, our speakers discuss novel research applications of atomic force microscope-based dynamic mechanical analysis (AFM-nDMA).

Watch to learn about how AFM-nDMA makes it possible for researchers to perform dynamic modulus determination (storage modulus, loss modulus, and loss tangent) with a wide-frequency range that is directly comparable to bulk DMA, but with the nanometer level resolution of AFM.

This capability is discussed, at length, using both case study and example analytical explorations.

In this webinar, Prof. Nakajima shares the pioneering work that he and his team have done to investigate the viscoelastic properties of heterogeneous rubber materials. Due to its frequency and temperature control capabilities, they used AFM-nDMA to validate time-temperature superposition (TTS) principle within microstructured domains. A rubber vulcanizate and a filler-reinforced rubber were studied as model samples. An interesting nanoscale heterogeneity in the rubber matrix was observed, which may imply the breakdown of the time-temperature superposition principle due to the heterogeneous nature of the glass transition.

Additionally, Bede Pittenger, Ph.D., discusses the work done at Bruker to optimize and validate the AFM-nDMA method. The technique is covered in detail along with examples to show its capabilities in both mapping at a single frequency and collecting spectra at user-specified points that are co-located with other mechanical property maps.

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This webinar was presented on: October 29, 2019